[RASMB] Lamp Intensities on Analytical Ultracentrifuges
John E Harlan
john.e.harlan at abbott.com
Fri Jun 1 11:49:09 PDT 2007
I am starting to have some problems with rapidly decreasing lamp
intensities on my analytical instruments. Within about 1 month of
moderate use after my service people were in (they cleaned the optics
while checking other things), I find the noise in my velocity absorbance
scans is quite bad. When I check the intensities I find maxima at 230nm
to be 8300 for an XLA and 13000 for an XLI, well below the 20000 to 30000
I should find for a well functioning instrument.
I have two questions:
1) What could cause such a rapid decay of performance. I suspect oil
leaks fouling the optics (I have observed droplets in the can on at least
one occasion). I understand alignment can also cause problems. Is there
something else to ask my service people to check?
2) I have heard that people that have upgraded to a turbo-molecular
vacuum pump have been quite pleased with performance. Can this upgrade
help keep my optics clean, if indeed that is the problem?
Thanks for your help in advance.
John
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