[RASMB] torque strength
Ariel Lustig
ariel.lustig at bluewin.ch
Thu Nov 17 07:05:00 PST 2005
Hi Karen and colleagues,
I can tell you only from my own experience how I treat this problem. First of all I use only sapphire windows,
since at the end they are cheaper then many broken quartz windows. Why broken ? my cell-stuff is very old so
Epoxy centerpieces (alum-filled and charcoal-filled) swell slowly and became a bit convext on both flat side , so I
even install (not too easy) in case of the bad once DS-window gaskets between the window and the centerpiece.
as it is obligatory for metallic centerpieces!!
Sure that in case of metllic centerpiece the torque strength is more crucial since lack of elasticity you break easier
the window just during closing the cell (not the centerpiece as you wrote ,Karen ! ) so 130 torque -units should be enough. A probleme may be the temperature, I torque the cell at the (coldest) temperature the run is planed , independend if I fill the cell at room temp.( if the sample allows it). The idea is to prevent shrinking later of the centerpiece....and leaking. A bit tolerance for higher temp. is still given with 130 t.
The Epoxy once "suffer" more tolerance, so 120 -140 is OK.
With time usually one gets the feeling witout looking on the torque dial especially using Epoxy once , according the
flexibility.
I don't believe that the torque instrument is a so precise instrument and unic by all users !!!
It may happen (I believe at most of you) that the screw-ring -gasket do not lie properly on top of the upper window- holder (catched in the winding or an alien element is between) breaks , and as response you may read a high torque
dial but in realty the centerpiece is not pressed to the windows.
Just returning to centerpiece break during a run , usually happens with quartz widows. First you have a leak
in one sector (may be evaporation true the filling screw), the filling hight liquid remain much higher as in the other sector, then the midle strap breaks and also
mostly the quartz window. (Saphire even at max.speed never break.)
yours...ariel
!
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