[RASMB] acetonitrile
Stephen Harding
Steve.Harding at nottingham.ac.uk
Tue Sep 20 08:08:52 PDT 2011
Dear Andrew and Ariel
Tom Laue and myself have recently been having a private discussion about this after some epon based centerpieces were (very!) worse for wear after exposure to dimethylacetamide.
As Ariel says, Kel-F double sectors have been reliable at modest temperatures but Beckman don't make them any more. Probably aluminium (not Al-epon) or titanium would do instead, but best to test them with the solvent in a beaker overnight.
If anyone not working on organics have any old ds KelF's (even old 30mm's) they'd like to get rid of or exchange for epons or even sell please let us know!
All best
Steve
_____________________________________________________________
Steve Harding, National Centre for Macromolecular Hydrodynamics, University of Nottingham, Sutton Bonington LE12 5RD, UK. Tel: +44(0) 115 951 6148 (fax 6142); Mob: +44(0) 78110 90635; http://www.nottingham.ac.uk/Biosciences/People/steve.harding; http://www.nottingham.ac.uk/ncmh (next year is 25th anniversary!)
________________________________
From: rasmb-bounces at rasmb.bbri.org [rasmb-bounces at rasmb.bbri.org] On Behalf Of Ariel Lustig [ariel.lustig at bluewin.ch]
Sent: 20 September 2011 15:20
To: rasmb
Subject: [RASMB] acetonitrile
Dear Andrew and & colleagues,
ten years ago, when I was still active in my AUC lab (now retired), when I had
a solvent where I do not know if it attacks a certain centerpiece, I took a piece of an old not more usable centerpiece (or other AUC labs gave me such a piece),
and put it in a vessel with the liquid fo one until 10 days and prooft if there are no sign of swelling or other attacks...if not I permit myself to use it.
In any case I had also all kinds of Kel-F centerpieces that are usually resistant except
Flour components...yours ariel
ariel.lustig at bluewin.ch<mailto:ariel.lustig at bluewin.ch>
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